If inhaled if breathed in, move person into fresh air. Cyclohexanone, a colorless liquid is a cyclic ketone. This material does not contain any class 1 ozone depletors. Eyes if material gets into eyes or if fumes cause irritation, immediately flush eyes with plenty of water until chemical is removed. Majority of the cyclohexanone synthesized is utilized as an intermediate in the synthesis of nylon. Safety data sheet cyclohexanone hill brothers chemical. The following list contains the material safety data sheets you requested. Dry powders can build static electricity charges when subjected to the friction of transfer and mixing operations. Organic chemistry lab reportsynthesis of cyclohexanone.
Show this safety data sheet to the doctor in attendance. Specific target organ toxicity single exposure no data available acute inhalation toxicity breathing difficulties. Material safety data sheet cyclohexanone msds section 1. Cyclohexanone ld50 1544 mgkg rat ld50 947 mgkg rabbit lc50 8000 ppm rat 4 h toxicologically synergistic products no information available delayed and immediate effects as well as chronic effects from short and longterm exposure irritation causes eye burns. It is an important building block for the synthesis of a variety of organic compounds. The information given is designed only as a guidance for safe handling, use, processing, storage. The information in cameo chemicals comes from a variety of data sources. The cyclohexanone is extracted into methylene chloride. Carefully add cyclohexanone, drop wise, to the small test tube until the balance shows a mass of 0. Use of the information, documents and data from the echa website is subject to the terms and conditions of this legal notice, and subject to other binding limitations provided for under applicable law, the information, documents and data made available on the echa website may be reproduced, distributed andor used, totally or in part, for noncommercial purposes provided that echa is. With larger ingestions there is potential for systemic t oxicity from gastrointestinal absorption and decontamination is suggested, keeping in mind that aspirat ion is still a concern. The mixture was cooled to 0c with an ice bath and pyrrolidine 1. Print pdf page for determination of zinc by the zincon zincover 5 method. Cyclohexanone is slightly soluble in water and miscible with common.
Preparation of cyclohexanone 23 online edition for students of organic chemistry lab courses at the university of colorado, boulder, dept of chem and biochem. First aid measures general advice move out of dangerous area. Sigmaaldrich 3050 spruce street saint louis mo 63103 usa. Identification of the substancemixture and of the companyundertaking 1. It is a colorless, oily liquid with an acetone like smell. In view of its moderate vapor pressure and low adsorption to soil, it would be expected to volatilize from surface soil. The following list contains the material safety data sheets. Collect contaminated fire extinguishing water separately.
Potassium permanganate safety data sheet according to federal register vol. The products are useful as gamma secretase inhibitors, or as intermediates in the synthesis of other gamma secretase inhibitors. Online edition for students of organic chemistry lab. Chemtrec 8004249300 outside usa 7035273887 1216 6th ave n kent wa 98032 phone. Safety data sheet cyclohexanone hill brothers chemical co. Iarc no component of this product present at levels greater than or equal to 0. Irritating to skin sensitization no information available. Jun 06, 2018 the synthesis of cyclohexanone is a simple procedure that uses acetic acid, sodium hypochlorite, hypochlorous acid, ether, sodium chloride, sodium carbonate and cyclohexanol. Fire residues and contaminated fire extinguishing water must be disposed of in accordance with local regulations. The synthesis is done by simply adding the acetic acid and sodium hypochlorite, which is also known as hypochlorous acid to.
Compare and contrast your ftir versus the literature ir for the starting material and the product see below. Exposure controlspersonal protection engineering controls. The co stretch on the cyclohexanone spectrum and show the absence of the alcohol stretches. Cyclohexanone is readily biodegradable according to aerobic screening tests and. Cyclohexanone material safety data sheet cas no 108941. Cyclohexanone 2,4dinitrophenylhydrazone santa cruz. To salt out the cyclohexanone, add to the distillate 0. Safety data sheet creation date 14sep2009 revision date 29oct2018 revision number 4 1. Buy your topgrade cyclohexanone online from reagent, a leading uk chemical supplier with over 40 years experience. A blank cell indicates the fabric has not been tested. Safety data sheet northwest missouri state university. Ensure all equipment is electrically grounded before beginning transfer operations. On a balance, tare a small test tube that has been placed in an empty 50 to 100ml beaker for stabilization. The bioconcentration factor bcf for cyclohexanone can be estimated to be 2.
Cyclopentanone material safety data sheet cas no 120923 sds. Cyclohexanone is estimated to be highly mobile in soil. Always wear recommended personal protective equipment. Identification product name potassium iodide cat no. India veritas house, 70 mint road, fort, mumbai 400 001. Although data are lacking, it may also undergo direct photolysis on the soil surface. It may be absorbed through the skin with symp toms similar to that of ingestion. Cyclohexanone is the organic compound with the formula ch 2 5 co.
Safety data sheet according to 29cfr19101200 and ghs rev. Provide exhaust ventilation or other engineering controls t o keep the airborne concentrations of vapors below their respective threshold limit value. Not classifiable as to its carcinogenicity to humans cyclohexanone reproductive toxicity overexposure may cause reproductive disorders bas ed on tests with laboratory animals. Follow the osha respirator regulations found in 29 cfr 1910. Material safety data sheet cyclohexane msds number. Make sure to discuss and label the oh stretch and the co stretch on the cyclohexanol spectrum.
If medical advice is needed, have product container or label at hand keep out of reach of children read label. Cyclohexanone is readily biodegradable according to aerobic screening tests and therefore would be expected to biodegrade in soil. Information in this sds is from available published sources and is believed to be accurate. Place a glass thermometer into the beaker and measure the temperature of the mixture.
Potassium iodide revision date 29oct2018 y2 indicates an exempt polymer that is a polyester and is made only from reactants included in a specified list of low concern reactants that comprises one of the eligibility criteria for the exemption rule. Page 6 of 8 msds t benzyl alcohol special remarks on other toxic effects on humans. Dissolving inorganic salts such as potassium carbonate or sodium chloride in the aqueous layer will decrease the solubility of cyclohexanone such that it can be completely extracted with ether. These intermediates are important in the manufacture of nylon6 and. Potassium nitrate safety data sheet according to federal register vol. This material does not contain any hazardous air pollutants. Uses advised against food, drug, pesticide or biocidal product use details of the supplier of the safety data sheet. One of the methods reported for its synthesis is by the palladium catalyzed hydrogenation of phenol. This colorless oil has an odor reminiscent of that of acetone. Sds of cyclohexanone, safety data sheets, cas 108941. P210 keep away from heat, sparks, open flames, hot surfaces. Sigmaaldrich c102180 page 1 of 6 sigmaaldrich material safety data sheet version 4.
The hazard fields include special hazard alerts air and water reactions, fire hazards, health hazards, a reactivity profile, and details about reactive groups assignments and potentially incompatible absorbents. Wear appropriate protective clothing to prevent skin exposure. A novel process for preparing cyclohexanone derivatives of formula i is described. Over time, samples of cyclohexanone assume a yellow color. If irritation persists, get medical attention immediately. Buy cyclohexanone leading chemical suppliers reagent. Cyclohexanone also known as oxocyclohexane, pimelic ketone, ketohexamethylene, cyclohexyl ketone or ketocyclohexane is a six carbon cyclic molecule with a ketone functional group. The molecule consists of sixcarbon cyclic molecule with a ketone functional group. May cause symptoms listed under inhalation, dizziness, fatigue, tremors, permanent central nervous system. Potassium carbonate anhydrous certified acs revision date 18sep2018 disclaimer the information provided in this safety data sheet is correct to the best of our knowledge, information and belief at the date of its publication. Page 4 of 8 msds t benzyl alcohol lightresistant containers. Aug 03, 2009 the molar mass of cyclohexanone is 98.
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